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PMID: 19795853 Published · ppublish English Journal Article Research Support, N.I.H., Extramural Research Support, Non-U.S. Gov't Research Support, U.S. Gov't, Non-P.H.S.

6-s-cis Conformation and polar binding pocket of the retinal chromophore in the photoactivated state of rhodopsin.

Journal of the American Chemical Society ·Vol. 131 ·No. 42 ·2009-10-28 ·Pages 15160-9

Ahuja S, Eilers M, Hirshfeld A, Yan EC, Ziliox M, Sakmar TP, Sheves M, Smith SO

Abstract

The visual pigment rhodopsin is unique among the G protein-coupled receptors in having an 11-cis retinal chromophore covalently bound to the protein through a protonated Schiff base linkage. The chromophore locks the visual receptor in an inactive conformation through specific steric and electrostatic interactions. This efficient inverse agonist is rapidly converted to an agonist, the unprotonated Schiff base of all-trans retinal, upon light activation. Here, we use magic angle spinning NMR spectroscopy to obtain the (13)C chemical shifts (C5-C20) of the all-trans retinylidene chromophore and the (15)N chemical shift of the Schiff base nitrogen in the active metarhodopsin II intermediate. The retinal chemical shifts are sensitive to the conformation of the chromophore and its molecular interactions within the protein-binding site. Comparison of the retinal chemical shifts in metarhodopsin II with those of retinal model compounds reveals that the Schiff base environment is polar. In particular, the (13)C15 and (15)Nepsilon chemical shifts indicate that the C horizontal lineN bond is highly polarized in a manner that would facilitate Schiff base hydrolysis. We show that a strong perturbation of the retinal (13)C12 chemical shift observed in rhodopsin is reduced in wild-type metarhodopsin II and in the E181Q mutant of rhodopsin. On the basis of the T(1) relaxation time of the retinal (13)C18 methyl group and the conjugated retinal (13)C5 and (13)C8 chemical shifts, we have determined that the conformation of the retinal C6-C7 single bond connecting the beta-ionone ring and the retinylidene chain is 6-s-cis in both the inactive and the active states of rhodopsin. These results are discussed within the general framework of ligand-activated G protein-coupled receptors.

MeSH Terms
Binding Sites Cell Line Humans Magnetic Resonance Spectroscopy Models, Molecular Molecular Structure Mutation Photochemical Processes Protein Structure, Tertiary Retinaldehyde/chemistry,metabolism Rhodopsin/chemistry,genetics,metabolism
Chemicals
Rhodopsin Retinaldehyde
Authors & Affiliations
8 authors, click to expand affiliations / ORCID
Ahuja Shivani
Department of Physics and Astronomy, Stony Brook University, Stony Brook, New York 11794-5215, USA.
Eilers Markus
Hirshfeld Amiram
Yan Elsa C Y
Ziliox Martine
Sakmar Thomas P
Sheves Mordechai
Smith Steven O
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Article Info
Journal
Journal of the American Chemical Society
Abbr.
J Am Chem Soc
ISSN
1520-5126
Published
2009-10-28
Pages
15160-9
Language
English
Region
United States
NLM ID
7503056
PMCID
PMC2783296
Subset
IM
Grants
NCRR NIH HHS · S10 RR13889 · United States
NIGMS NIH HHS · R01 GM041412-16 · United States
NIGMS NIH HHS · R01 GM041412-17 · United States
NIGMS NIH HHS · R01 GM041412-18 · United States
NIGMS NIH HHS · R01 GM041412-15 · United States
NIGMS NIH HHS · R01 GM041412 · United States
NIGMS NIH HHS · GM-41412 · United States
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