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PMID: 11777 Published · ppublish English Journal Article

Preparation of fully active ficin from Ficus glabrata by covalent chromatography and characterization of its active centre by using 2,2'-depyridyl disulphide as a reactivity probe.

The Biochemical journal ·Vol. 159 ·No. 2 ·1976-11-00 ·Pages 221-34

Malthouse JP, Brocklehurst K

Abstract

1. Fully active ficin (EC 3.4.22.3) containing 1 mol of thiol with high reactivity towards 2,2'-dipyridyl disulphide (2-Py-S-S-2-Py) at pH4.5 per mol of protein was prepared from the dried latex of Ficus glabrata by covalent chromatography on a Sepharose-glutathione-2-pyridyl disulphide gel. 2. Ficin thus prepared is a mixture of ficins I-IV and ficin G, in which ficins II and III predominate. The various ficins exhibit similar reactivity characteristics towards 2-Py-S-S-2-Py. 3. Use of 2-Py-S-S-2-Py as a reactivity probe demonstrates (a) that in ficin, as in papain (EC 3.4.22.2), the active-centre thiol and imidazole groups interact to provide a nucleophilic state at pH values of approx. 6 additional to the uncomplicated thiolate ion that predominates at pH values over 9, and (b) a structural difference between ficin and papain that leads to a much higher rate of reaction of 2-Py-S-S-2-Py with ficin than with papain at pH values 3-4. This difference is suggested to include a lack in ficin of a carboxyl group conformationally equivalent to that of aspartic acid-158 in papain. 4. The high electrophilicity of the 2-Py-S-S-2PyH+ monocation allows directly the detection of the exposure of the buried thiol group of ficin at pH values below 4.

MeSH Terms
2,2'-Dipyridyl Arginine/analogs & derivatives Benzoylarginine Nitroanilide Binding Sites Chemical Phenomena Chemistry Chromatography, Agarose Chromatography, Ion Exchange Disulfides Endopeptidases/isolation & purification Ficain/isolation & purification Hydrogen-Ion Concentration Hydrolysis Kinetics Mercaptoethanol Nitrophenols Plants/enzymology Protein Denaturation Pyridines
Chemicals
Disulfides Nitrophenols Pyridines 2,2'-Dipyridyl Mercaptoethanol Benzoylarginine Nitroanilide Arginine Endopeptidases Ficain
Authors & Affiliations
2 authors, click to expand affiliations / ORCID
Malthouse J P
Brocklehurst K
References (32)
32 references, click to expand
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Article Info
Journal
The Biochemical journal
Abbr.
Biochem J
ISSN
0264-6021
Published
1976-11-00
Pages
221-34
Language
English
Region
England
NLM ID
2984726R
PMCID
PMC1164109
Subset
IM
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